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<div>　　<strong>多歧管旋轉(zhuǎn)蒸發(fā)儀</strong>是一種用于制備薄膜的實驗設(shè)備。它的工作原理是在真空環(huán)境中，將待沉積材料加熱至升華溫度，使其蒸發(fā)并在襯底表面形成薄膜。該設(shè)備包含一個多歧管，在多個孔洞中放置不同的材料塊，并通過旋轉(zhuǎn)將它們帶到材料加熱區(qū)域。加熱區(qū)域由電阻絲或電子束提供熱源，當(dāng)材料達(dá)到升華溫度時，它們會開始蒸發(fā)，經(jīng)過冷凝后在襯底上沉積成薄膜。</div><div>　　<strong><a href="http://m.taimeizg.com/Products-38010829.html" target="_blank">多歧管旋轉(zhuǎn)蒸發(fā)儀</a></strong>的操作步驟：</div><div>　　1、準(zhǔn)備工作</div><div>　　連接冷卻水：將冷卻水（自來水或低溫冷卻循環(huán)裝置）連接到冷凝器上，以增加冷卻效果。</div><div>　　準(zhǔn)備主機(jī)和真空泵：確保主機(jī)各部件齊全且功能正常，并準(zhǔn)備好真空泵及注滿水的水箱。</div><div>　　2、開始操作</div><div>　　調(diào)整主機(jī)高度：調(diào)節(jié)主機(jī)高度，使加熱浴面高于或平于旋轉(zhuǎn)瓶液面，確保加熱效率。</div><div>　　固定旋轉(zhuǎn)瓶：裝上旋轉(zhuǎn)瓶并用夾子固定好，如有防濺接頭，先接上再裝旋轉(zhuǎn)瓶。</div><div>　　3、設(shè)置參數(shù)</div><div>　　設(shè)定旋轉(zhuǎn)速度和加熱溫度：根據(jù)實驗需求設(shè)定適當(dāng)?shù)男D(zhuǎn)速度和加熱溫度，以優(yōu)化蒸發(fā)效果。</div><div>　　開始旋轉(zhuǎn)和加熱：啟動旋轉(zhuǎn)開關(guān)和加熱開關(guān)，調(diào)節(jié)轉(zhuǎn)速和調(diào)溫旋鈕，開始試運行。</div><div>　　4、進(jìn)行蒸餾</div><div>　　關(guān)閉放氣閥：關(guān)閉加料閥，打開真空泵開始減壓進(jìn)行蒸餾。</div><div>　　監(jiān)控蒸餾過程：定期檢查旋轉(zhuǎn)瓶中液位變化和濃縮進(jìn)度，確保蒸餾順利進(jìn)行。</div><div>　　5、結(jié)束操作</div><div>　　停止旋轉(zhuǎn)和加熱：關(guān)閉旋轉(zhuǎn)開關(guān)和加熱開關(guān)，升起主機(jī)使旋轉(zhuǎn)瓶離開加熱浴。</div><div>　　關(guān)閉真空泵：打開放氣閥放壓，關(guān)閉真空泵及冷卻水。</div><div>　　6、收集樣品</div><div>　　取出旋轉(zhuǎn)瓶：從旋轉(zhuǎn)瓶中取下已濃縮的樣品，并進(jìn)行后續(xù)分析或儲存。</div><div>　　7、清理維護(hù)</div><div>　　清潔設(shè)備：實驗結(jié)束后，清潔旋轉(zhuǎn)瓶和設(shè)備，確保下次使用時的良好狀態(tài)。</div> 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